Six of the metal items recovered from Tomb 1 at Fassuta were sampled and analyzed. The chemical analysis revealed that five of the items were made of tin bronze and one item, a shaft-hole axe, was made of arsenic copper with lead. Interestingly, it was noted that during the Middle Bronze Age levels of lead at 4% or more are only found in this type of axe and in the duckbill-shaped axe. It can be said that the metallurgical profiles of the objects from Fassuta well fit our knowledge of archaeometallurgy of MB I (MB IIA).